Microstructural assessment of cubic InN film grown by molecular beam epitaxy
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Title Microstructural assessment of cubic InN film grown by molecular beam epitaxy
Creator Papaporn Jantawongrit
Contributor Sakuntam Sanorpim, Chanchana Thanachayanont
Publisher Chulalongkorn University
Publication Year 2551
Keyword Molecular beam epitaxy, Microstructure, Thin films
Abstract In the thesis, structural modification and crystal quality of cubic InN (c-InN) films grown on GaAs (001) substrates by molecular beam epitaxy have been systematically investigated and analyzed. The effects of growth conditions, namely In- and N-rich conditions, are established. Based on high-resolution X-ray diffraction, the result demonstrates that all the InN grown films have a cubic structure. On the other hand, electron diffraction (ED) pattern and cross-sectional transmission electron microscopy (TEM) micrographs demonstrate that the InN grown films contain a high density of stacking faults (SFs) parallel to (111) planes. Besides, the density of SF and twin defects decreases with the distance from the interface of c-InN/GaAs. No different type of single diffraction spots on the ED pattern was observed. On the other hand, TEM micrographs the ED patterns demonstrate that the c-InN films exhibited a transition from cubic to mixed cubic/hexagonal phase under N-rich growth conditions. In addition, µ-Raman scattering spectra obtained from these InN layers confirmed the existence of a structural modification from cubic to mixed cubic/hexagonal phase in microstructure of the N-rich layers, which exhibit higher hexagonal-phase incorporation than that of the In-rich layers. Our results suggest that the growth condition is a key parameter in the growth of high cubic phase purity c-InN films with lower incorporation of single-crystal h-InN.
URL Website cuir.car.chula.ac.th
Chulalongkorn University

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